TGA-601熱重分析儀檢測參數的確定

山13%3U1akμcAVol, 13 No. 32000Ae60AGUANGDONG ELECTRIC POWERJun.2000TAA±a9A007290X“2000903-000603TGA-601EE00-0l09aa2IEyμAE「ATEey2Uf-C8007af"1aeiucAHEONeNDMiEuf-1afs1a0Y 510600E000aa°TTGA601E0-0100uAa1ioua-f"y·0160 Ai HAeuNeEy4YE00AEAA0UE0j￠0-·02AEjc0·02AEμ DAHAi2a2Ey12a6AE0c0E÷110EI2a%· ETuAEtIYE10n2-C0AE0cCE;D0 AUTET'icx031作BA0 AuaieilyE-fDEoy正Ey1a隨10,道xkEE-1aBAE1 ax=DSAES10± OEC Ia. BAEA914i0DAA2aE8100EE00160c0E-0￡x0·0Ex0-·0E2EyE0D-0AaA￡9TQ533.2TAT×± eESAef9ADetermination of testing parameters of TGA-601 thermogravimetric analyzerLI Shu-iief-QIAN Yi-huaE Guangdong Power Test Research Institutef -Guangzhou 510600f-ChinazoAbstracte In light of the structural features of TGA-601 thermogravimetric analyzer and through analysis of a vast amount offea dataf-testing parameters such as inner moisture volatile matterfetc are redeterminedf which remedies the de-fects in configuration and testing method of the analyzer and gives further play to its advantages of stable performance andhigh automation level. The determination of calibration factors also improves the accuracy of test results as well as the workKey words%thermogravimetric analyzer E>moisture contentEmash contentEwvolatile matterEodetermination of parametersAAuAH iE E34OFOi HA TGA-601 EE00-0lo0cf- bfCEEIi FEh2uAOH OAjCEE Ii E2uA0H OA2kuE12aA0÷00A0U1a0T602 aEOjEfaAU20÷011b10AA0眶。.BE-0C0E100、62a001y910,8TAx-TAeip3c0 olHl39IEEliEjfA X0:0TA1§14100~3-EE￥AE4Aa00ysiE0AE20x÷UEAE1000℃21TA正『0E官±4℃E"aE1EUAE2x÷10621 CH OEOUEU00110iA0Tao. 1 mgf-2aAix4E-ETa003%E"1 sigmaf-ninert AHiE1Esaia' GuAEuNe-y2-2"EuNe2TEyOA%Y AA101uy0samplefqEooFo-0+o1 i OFo i Eo INOFEO iE4-1y3o *exy ASTM Ee/EE-4Bia2TEy0+i 1 20e101u TODDHA2uA°2x°0E-c0A0 CA+ 3yAEODAV4% AHA:0 SIADOAU100土ex4-“0BU620iiEHa1-E±-"ya^TENe06E00A00÷土EaaCAA9AuA00oipa101100±ex啊E8-0c1@ A ASTM-MⅤA·“A0-·“E0T01±eA00jc0-c0μAi2a1bA÷E·1a°A00E.0μA12a%i2aa100 e+eA9Ou00210E0±129i2a00UoA·cuAE0 ilaoD￡x0·0pAi2a0 PqUoDNICEi2LE30￡￡A￡ciaa0u0±e330±exNAr￥A-0E∞0-c·000UA0±0μAA￥A-0 Di*f ANub中國煤化工6×00420TGA601E000160c00Iu=μA0H0A￡~±0aAEcCNMHA°0E0a^a0UTE8-O2a'E+AoNu2n*oNOr9iE80E3AuAA30f-20-02a 62101 TGA-601 EtUV-U lo Eu ia@HA ASTM-們E土ANu|eEN-00°0-c-02aE±AN0. BIAIA MVA印Ne“2E0A0UT01°GB··“ DDHAA2a±N,-EE12aA0xkE-E0Ei2a￡n0ae0 aTOAC u4YOCRE÷10pa~0 DAE-T14iE0aE0EU兩嫩據2 allEy i￡HU 3 EUATEe2UuEfQTGA-601 EE00-0100C1i2a2lEyuAEr"±「1ASTM-MVA1·A03E0ac^AEy"℃-18E短/ min EOEVlA/001A″E/℃olaA自±30E短/min9a00/%a03E/miE8-0|pμE0Bco0000.0ip750±2 ASTM-MVA·“士eAP2a010eex)0μAE%±30--“0DA.·A"M28i2a0uA啊土%E8·0EA·0Ey∞00EA·0Ey∞0·c-00EA·0Ey土 bAotAuf m.2tEAECue v.EG712.0210.03E2auμEpμ2a0μ2opEu2a0μ20u831.012110002a2.9242.63+0.3814.16+2.6110004a2.241.8537,62+0,4919.68-1.74859.022l10005a2.939332.52+0.3316.48+0.412.712E0-0V4i2a2IEyHAE-110005a2.6+0.022.370.010 aATHAl⑥·OEcO00E0T>0 A NUHAAUOUE-0iEEuoolTAi"NS-hEn20eA Wa iE-EaE80oFEoN1AiDiOUiIASEIA E800oN1A200E0TA64TA2aEEY±020·02uAEi2a21 EyHAE·qD600105~110℃ HAIASEIA2 AAUYE￥EA0UE0EaBANu0o、E0μA16b0±a￡Ec0,62ET甲EAU0UAoOD0-0EC0, AoODEuODi EE). B lATAleEEv4E8-OHAo-Ai oeA uAA@,"3INEQiva110D102-2 i-HAAsEOf-FEaoDiolioEOUi OFEoOD-CEuos lHAD-OVaj C9THE00·0}°oEUE￡0aμA2Bo￡0·020AEuA2aq0UA°OE0E2~030aD02,12100e0-A022a0E士EEY0xE,2aAT了A020°ace2n12ux1A+0y20N1A6,01019.eE200BeE2apA36E1010100±exGB212i1991091a們 HAEuNe300.BAap,Er.“214A02c0096891000+Ae”s112.47±0.050OU EOTH FEoOD, EOTW/OEAiaE-0oODuFEo+Emnf-AQ HAvi2ava uA- TOFE, BE-10 110008 eAe"&"s,sEd0.67±0.052002ye0U0a000T6E0a土A÷00,8N》N22A×E9.E2Ex÷1909.160A2A0,A20y=9地N00:0B0EA00EAE·T2aEyE0- ASTM-MVA··”000FEoA-EUOE BE"highf@ATa Eie"med 0 TA 3E DA-100 COaECOO1A9ODOD uAoicFEluiOA00U 500 COOC40±40aeEs￡“EU3EAoμAN6T0A0BEaNE"00Ea,1Ay回0500℃E,0au800士08010E30800+80A0008E2A,0隨自EEE自9E5-、E‰面1啊0± DONee-Eμ NeEy4YEc±3E1v42j2i¨ 1yEy4Y1AiμA2T00DEEa=0.05￡-x00ESE f=7E-t vi NeuAAUgOW ta=2.365E-t vi neHA l3中國煤化工AA1t1=2.3312tl0土%ETA0·0A°uA,-1"E1-E±0-c·006A°μAOD。xe0E000°.cE:08a020A9AμATBD010EE000-0.02 uAEECx IODE!μkEo200300400500600700800OAVAUOHuA0, +e0B02-xiAU-OHA HAloDoj>0溫度/℃c·02uAEU2a6b°TiaT￡n220x2ax10161和AE2a”0·c·0μAIE10A^ OODNIAUCxOuAx0AUaU6-0g“90±100CIAiv2 AoODivEaNie"CaCO3ECuA-0%acuI040040E7 mini,u4Y土4OcCE÷A110i10pa2-0·c·02AEA×kE2a"E360u2 aAi latic2aAEaE00E.2aT“002AEA10 Cni Once土A02aAE土A0520E0TGA601E0.0T60c0DA49AEBrc6b￡1A0A0U0Ea.EaEk0a0間A00 TuiaE-A01±20a2aA1y91006A-AUaAc0a|eE2cE3A096￡-00土 UAaee.0aE3EμAN[0E土20TANu2±N》E2E0cCE0E10-020x÷-iit No-ETuEOf-0i3E, BAoic, B, EA ,0"% uFE 31D00D140UaUo, C210ef-140-2Ux:1yiE-ia, BxinB206啊00a00c66￡10 K ASTM-MVA·0B。0s哐i￡a0}A±aA-TA1a900℃E印Nea10始02a100E600℃EyTA750℃uA02EyTA0±5EAT0E300℃, ay Ey IA500℃E-E960U0E500℃EyTA.810℃A2EyTA0-2EyA土a±「5國V￡pABA·”2a00e土 ex OHuAgO土E%96μA2a“a100±f42土6AooAl10002a16.1316.77±0.32±4AE@uADA-2-“i2a0u0e±exOμuA啊O±%110004a21,021,42±0.34±eAAE"ME0E”A0“AE0￡A2exou20ul1000822.923.12±0.340.15712,0212.2412.3412,6212.97±0.250.35712.02134.5834.72±0.69014831.0121.9412.612.8512.70±0.22+0.15945.0211.247.177.24±0.10±5Ey4Y%-tiNe.HAi°uAa=0.052f859.0222.9413.3513.7513.82±0.20-0.0=3￡-tn=3.182|t|=2.66121t